|
KIML5717 | Separation and Enrichment Techniques | 3+0+0 | ECTS:7.5 | Year / Semester | Fall Semester | Level of Course | Second Cycle | Status | Elective | Department | DEPARTMENT of CHEMISTRY | Prerequisites and co-requisites | None | Mode of Delivery | | Contact Hours | 14 weeks - 3 hours of lectures per week | Lecturer | Prof. Dr. Celal DURAN | Co-Lecturer | Prof. Dr. Celal Duran, , Prof. Dr. Ümmühan Ocak, Prof. Dr. Miraç Ocak, Doç. Dr. Celal Duran, Prof. Dr. Ömer Dalman, Pof. Dr. Hakan Alp, Öğr. Gör. Dr . Sinan Nohut | Language of instruction | Turkish | Professional practise ( internship ) | None | | The aim of the course: | Learning the separation and enrichment processes required prior to analysis |
Programme Outcomes | CTPO | TOA | Upon successful completion of the course, the students will be able to : | | | PO - 1 : | Learning generel enrinchement methods | | | PO - 2 : | Learning evaporation and liquid- liquid extraction | | | PO - 3 : | Learning precipitation, selective solving | | | PO - 4 : | Understanding electrochemical precipitation | | | PO - 5 : | Learning sorption, ion exchange and flotation | | | PO - 6 : | Learning enrichment methods before analysis | | | PO - 7 : | Learning separation and purification methods | | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), PO : Learning Outcome | |
General methods of enrichment techniques. Evaporation. Liquid-liquid extraction . Precipitation. Selective dissolution . Electrochemical deposition. Sorption and ion-exchange. Flotation. Freezing and zone melting. Enrichment techniques in gas and water analysis . Separation and purification, fractional precipitation , decomposing and dissolving , separation with hydroxide and sulfide , fluxes , extraction methods, ion exchange , supercritical extraction , chromotography. |
|
Course Syllabus | Week | Subject | Related Notes / Files | Week 1 | general methods of enrichment techniques. | | Week 2 | Evaporation, Liguid-liquid extraction | | Week 3 | Precipitation, Selective solving | | Week 4 | Electrochemical precipitation, Sorption and ion exchange | | Week 5 | Flotation. Freezing and melting | | Week 6 | Enrichment techiques in gas and water analysis | | Week 7 | Separation and purification, Fractional precipitation | | Week 8 | Digestion before separation | | Week 9 | Mid-term exam | | Week 10 | separation with hydroxide and sulfide | | Week 11 | Melting, extraction methods | | Week 12 | Ion exchange | | Week 13 | Electrophorese | | Week 14 | Supercritical extraction | | Week 15 | Chromatograpyh | | Week 16 | Final exam | | |
1 | Kılıç, Esma, Köseoğlu Fitnat, Analitik Kimya 2, Bilim Yayıncılık | | |
Method of Assessment | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | Mid-term exam | 9 | 01/12/2023 | 1 | 50 | End-of-term exam | 16 | 22/01/2024 | 1 | 50 | |
Student Work Load and its Distribution | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | Yüz yüze eğitim | 3 | 14 | 42 | Sınıf dışı çalışma | 4 | 14 | 56 | Laboratuar çalışması | 0 | 0 | 0 | Arasınav için hazırlık | 5 | 8 | 40 | Arasınav | 1 | 1 | 1 | Uygulama | 0 | 0 | 0 | Klinik Uygulama | 0 | 0 | 0 | Ödev | 1 | 1 | 1 | Proje | 0 | 0 | 0 | Kısa sınav | 0 | 0 | 0 | Dönem sonu sınavı için hazırlık | 6 | 4 | 24 | Dönem sonu sınavı | 1 | 1 | 1 | Diğer 1 | 3 | 8 | 24 | Diğer 2 | 0 | 0 | 0 | Total work load | | | 189 |
|