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| EAK6003 | Supercritical Fluid Chromatography and Extraction | 3+0+0 | ECTS:7.5 | | Year / Semester | Fall Semester | | Level of Course | Third Cycle | | Status | Elective | | Department | ANALYTICAL CHEMISTRY IN PHARMACY | | Prerequisites and co-requisites | None | | Mode of Delivery | | | Contact Hours | 14 weeks - 3 hours of lectures per week | | Lecturer | -- | | Co-Lecturer | | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | Students learn supercritical fluid chromatography and extraction methods |
| Programme Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | PO - 1 : | Have knowledge about method optimization processes for the use of supercritical fluid chromatography in the analysis of active pharmaceutical ingredients | 1,3,5,6 | 1, | | PO - 2 : | Understands the importance of supercritical fluids in terms of green chemistry | 1,3,5,6 | 1, | | PO - 3 : | Learn the applications of supercritical fluids in the isolation of compounds of economic importance | 1,3,5,6 | 1, | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), PO : Learning Outcome | | |
| In this course, students will learn about supercritical fluid chromatography and extraction, which has recently been highly emphasized and plays an important role in biomedicine and food analysis. |
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | Introduction | | | Week 2 | Supercritical Fluid Extraction | | | Week 3 | Supercritical Fluid Extraction | | | Week 4 | Definition of Supercritical Fluids | | | Week 5 | Supercritical Fluid Selection | | | Week 6 | Features of Supercritical CO2 | | | Week 7 | Resolving Power of Supercritical Fluids | | | Week 8 | Supercritical Fluid Extraction System | | | Week 9 | Mid-term exam | | | Week 10 | Supercritical Fluid Extraction System | | | Week 11 | Advantages of Supercritical Fluid Extraction | | | Week 12 | Advantages of Supercritical Fluid Extraction | | | Week 13 | Disadvantages of Supercritical Fluid Extraction | | | Week 14 | Application of Separation Technology with Supercritical Fluids | | | Week 15 | Uses of Supercritical Fluids | | | Week 16 | Final exam | | | |
| 1 | Larry M. Miller, J. David Pinkston, Larry T. Taylor, 2019, Modern Supercritical Fluid Chromatography: Carbon Dioxide Containing Mobile Phases John Wiley & Sons, Inc. DOI:10.1002/9781119626022 | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 25/11/2023 | 2 | 30 | | In-term studies (second mid-term exam) | 15 | 10/01/2024 | 2 | 20 | | End-of-term exam | 16 | 05/01/2024 | 2 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Yüz yüze eğitim | 3 | 14 | 42 | | Arasınav için hazırlık | 8 | 8 | 64 | | Arasınav | 2 | 1 | 2 | | Dönem sonu sınavı için hazırlık | 6 | 14 | 84 | | Dönem sonu sınavı | 3 | 1 | 3 | | Total work load | | | 195 |
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